DY501型

      電熱熔融設(shè)備

可4個(gè)樣同時(shí)熔融，自動(dòng)搖擺，自動(dòng)控制；

成型模具自動(dòng)加熱，自動(dòng)冷卻，自動(dòng)成型；

大屏幕中文顯示，過(guò)流過(guò)溫自動(dòng)報(bào)警切斷；

可自由設(shè)定加溫過(guò)程，預(yù)存多個(gè)加溫程序。

簡(jiǎn)介

X射線(xiàn)熒光分析對(duì)于粉末樣品，目前采用直接壓片法制備試樣較為普遍，但由于粒度、礦物、偏析等效應(yīng)的影響，勢(shì)必帶來(lái)分析誤差，降低元素分析的精密度與準(zhǔn)確度，樣品制備已經(jīng)成為一個(gè)主要的誤差因素。玻璃熔融法制成的試樣能消除試樣的粒度、礦物、偏析等效應(yīng)，同時(shí)也可降低樣品元素間的吸收和增強(qiáng)效應(yīng)，會(huì)明顯提高分析的精度和準(zhǔn)確度。對(duì)于ICP、AA和濕法化學(xué)分析手段，對(duì)于難溶樣品，熔融方法同樣是一種非常的制樣手段。

多年來(lái)國(guó)內(nèi)所采用的熔融設(shè)備均依賴(lài)進(jìn)口，價(jià)格非常昂貴，針對(duì)這種局面，本公司科研人員于2002年開(kāi)發(fā)完成了空白的DY501型電熱熔融設(shè)備。它吸取了當(dāng)今國(guó)際市場(chǎng)上同類(lèi)制樣設(shè)備的優(yōu)點(diǎn)，其主要性能達(dá)到甚至超過(guò)國(guó)外同類(lèi)產(chǎn)品。由于其優(yōu)異的性能和合理的價(jià)格，定將取代進(jìn)口產(chǎn)品，并使原來(lái)由于經(jīng)濟(jì)原因暫不用熔融設(shè)備的用戶(hù)也能使用它。DY501型電熱熔融設(shè)備的推出，定將迅速普及熔融制樣法，從而提高我國(guó)分析界制樣的水平，為各行各業(yè)帶來(lái)巨大的經(jīng)濟(jì)效益。

Brief Intoduction

Currently, powdered samples for X-ray fluorescence analysis are usually directly pressed into sample pieces. But that kind of sampling has become a major error factor impacting the precision and accuracy of the element analysis due to the granularity effect, mineral effect and segregation effect of the sample pieces. The bead fusion method can eliminate the granularity, mineral and segregation effects of the samples, and can reduce the absorption and enhancement effects between the elements in the sample, and hence evidently increase the precision and accuracy of the analysis. This bead fusion method is a perfect sampling method for ICP, AA, as well as for indissolvable samples in wet chemical analysis.

For many years, the fusion machine used in China were all imported from abroad at very high price. To fill up that gap in Chinese science and technology, the research and development personnel in our company developed the DY501 Electroheat Fusion Machine in the year 2002. This fusion machine absorbed the advantages of all the fusion machine of the same kind in the international markets, with key properties up to or even better than those of the overseas products. With its excellent performance and reasonable price, it will take the place of the imported products and can be affordable for the users which are currently not using fusion units just because of economic reasons. The popularization of the DY501 Electroheat Fusion Machine will rapidly promote the bead fusion method in China and hence improve the sampling quality of the element analysis, which can bring tremendous economic benefit for every industry or trade.

技術(shù)參數(shù)

加熱單元：3根雙螺旋單端硅碳棒；

溫度：1250℃，連續(xù)可調(diào)；

測(cè)溫單元：2根鉑銠熱電偶，測(cè)溫1600℃；

容量：同時(shí)熔融4個(gè)樣品（可根據(jù)用戶(hù)要求增加到6個(gè)）；

功率：6kw;

電源：380-415V,50-60Hz，三相;

尺寸（高×寬×深）：500mm×1217mm×500mm;

重量：115kg.

Technical Specifications

Heating unit: 3 pieces of double helix ,single-end, silicon carbide rod

Maximum Temperature: 1250℃,continuously adjustable

Temperature measurement unit: 2 pieces of platinum-rhodium thermocouple, with maximum measurable temperature 1600℃

Capacity: 4 samples simultaneously (maximum 6 samples if required by user)

Wattage: 6kw

Power supply: 380-415V,50-60Hz，three phase

Dimension(Height ×Width × Depth): 500mm×1217mm×500mm

Weight: 115kg

主要特點(diǎn)

◆采用CPU微機(jī)及PID控制技術(shù)，大屏幕中文顯示,菜單式操作；

◆雙螺旋硅碳棒加熱，鉑銠熱電偶測(cè)溫；

◆最多可同時(shí)熔融4個(gè)樣品（可根據(jù)用戶(hù)要求增加到6個(gè)）；

◆可預(yù)先自由設(shè)定最多達(dá)10個(gè)加熱制樣程序，其加熱過(guò)程，升溫速度，最終溫度，坩堝架搖擺時(shí)間、幅度、速度，冷卻時(shí)間，是否用風(fēng)扇，風(fēng)量大小等均可預(yù)先設(shè)定；

◆除熔融樣注入成型模具采用手動(dòng)外，其他均自動(dòng)控制，保證了樣品的一致性和均勻性，真正做到不同樣品僅是其成分不同而沒(méi)有其他不同；

◆坩堝及成型模具的支架采用耐高溫合金鋼制成,保證在高溫狀態(tài)下無(wú)任何化學(xué)反應(yīng)；

◆熔樣室蓋打開(kāi)裝置采用鏈輪杠桿結(jié)構(gòu)，操作輕松自如；

◆具有啟動(dòng)溫度報(bào)警，打開(kāi)熔樣室斷電保護(hù)；

◆具有過(guò)流、過(guò)溫?cái)嚯姳Ｗo(hù)并報(bào)警，并且過(guò)溫?cái)嚯姳Ｗo(hù)采用與加熱制樣獨(dú)立的熱電偶測(cè)溫，與加熱控制電路一起組成三重保護(hù)，使過(guò)溫?cái)嚯姳Ｗo(hù)更可靠。

Features

◆Applies CPU microprocessor and PID control technique, large screen Chinese display, and menu operation

◆Heating with double helix silicon carbide rod; temperature measured with platinum-rhodium thermocouple

◆Up to 4 samples can be fused simultaneously (maximum 6 samples if required by user)

◆Up to 10 customized heating programs can be preset; within the programs, the heating process, the temperature increase speed, the final temperature, the shaking time, shaking amplitude, and shaking speed of the crucible stool, the cooling time, whether to use fans, the air flow, and so on, all can be preset.

◆Automatic control in all the process except for the filling of the fusion sample, enabling the sameness and homogeneity of the sample; all samples are uniformly the same except for the differences in composition

◆The bracket of the crucible and the mould are made of high temperature alloy, which guarantees no chemical reaction in high temperature

◆Chain wheel lever structure is used in the opening device of the cover of the fusion room, trouble-free for user operation

◆With minimum start temperature alarm and power switch-off protection when the cover of the fusion room is open

◆Automatically switching off power and setting alarm for overcurrent and overheat; independent temperature measurement thermocouples are used for overheat protection and heating control; together with the heating control circuit, they can form treble protection of the system and can make the power switch-off protection for overheat more reliable.